Quinoline and phenanthroline preparation starting from glycerol via improved microwave-assisted modified Skraup reaction

Hanen Saggadi; Denis Luart; Nicolas Thiebault; Isabelle Polaert; Lionel Estel; C. Len

doi:10.1039/C4RA00758A

Journal articles

Quinoline and phenanthroline preparation starting from glycerol via improved microwave-assisted modified Skraup reaction

Hanen Saggadi ^{1, 2} Denis Luart ¹ Nicolas Thiebault ¹ Isabelle Polaert ² Lionel Estel ² C. Len ¹

1 TIMR - Transformation Intégrée de la Matière Renouvelable

2 LSPC - Laboratoire de Sécurité des Procédés Chimiques

Abstract : An efficient “green” modified Skraup reaction in neat water was developed using inexpensive, abundant and environmentally-friendly glycerol under microwave irradiation conditions. Starting from aniline derivatives, various quinolines were obtained in 10–66% yields. The use of nitroaniline led to the corresponding phenanthrolines in 15–52% yields, respectively.

Document type :

Journal articles

Domain :

Engineering Sciences [physics] / Chemical and Process Engineering

Complete list of metadatas

https://hal-normandie-univ.archives-ouvertes.fr/hal-02409872
Contributor : Isabelle Polaert <>
Submitted on : Friday, December 13, 2019 - 3:48:13 PM
Last modification on : Thursday, February 6, 2020 - 9:18:02 AM

Quinoline and phenanthroline preparation starting from glycerol via improved microwave-assisted modified Skraup reaction

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Quinoline and phenanthroline preparation starting from glycerol via improved microwave-assisted modified Skraup reaction

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