High-Density Octadecyl Chemically Bonded Core–Shell Silica Phases for HPLC: Comparison of Microwave-Assisted and Classical Synthetic Routes, Structural Characterization and Chromatographic Evaluation

Mélanie Mignot (1) , Alain Tchapla (2) , Olivier Mercier (3) , Nicolas Couvrat (1) , Séverine Tisse (1) , Pascal Cardinaël (1) , Valerie Peulon-Agasse (1)

1 SMS - Sciences et Méthodes Séparatives
2 Groupe de chimie analytique de Paris-Sud - Laboratoire d’Étude des Techniques et Instruments d'Analyse Moléculaire (LETIAM)
3 Interchim R & D

Domains: Chemical Sciences; Chemical Sciences; Material chemistry; Chemical Sciences; Organic chemistry; Chemical Sciences; Analytical chemistry

Mélanie Mignot, Alain Tchapla, Olivier Mercier, Nicolas Couvrat, Séverine Tisse, et al.. High-Density Octadecyl Chemically Bonded Core–Shell Silica Phases for HPLC: Comparison of Microwave-Assisted and Classical Synthetic Routes, Structural Characterization and Chromatographic Evaluation. Chromatographia, 2014, 77 (23-24), pp.1577 - 1588. ⟨10.1007/s10337-014-2802-x⟩. ⟨hal-01929987⟩